chloro(4-methylphenyl isocyanide)gold(I)

Base Information

Chemical Name:chloro(4-methylphenyl isocyanide)gold(I)
CAS No.:43067-30-7
Molecular Formula:C₈H₇AuClN
Molecular Weight:349.57
Hs Code.:

Synonyms:chloro(4-methylphenyl isocyanide)gold(I)

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Chemical Property of chloro(4-methylphenyl isocyanide)gold(I)

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Technology Process of chloro(4-methylphenyl isocyanide)gold(I)

There total 1 articles about chloro(4-methylphenyl isocyanide)gold(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 7175-47-5
4-methylphenyl isocyanide

: 43067-30-7
chloro(4-methylphenyl isocyanide)gold(I)

Guidance literature:: In dichloromethane; at 20 ℃; for 13.5h;
DOI:10.1021/jacs.6b02409

Reference yield: 90.0%

: 43067-30-7
chloro(4-methylphenyl isocyanide)gold(I)

: C₇H₄INZn*Li⁽¹⁺⁾*Cl^(1-)

: C₁₅H₁₁AuN₂

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/jacs.6b02409

Reference yield: 89.0%

: 43067-30-7
chloro(4-methylphenyl isocyanide)gold(I)

: 109-89-7
diethylamine

: [AuCl(C(NEt₂)(NHTol-p))]

Guidance literature:: In CH₂Cl₂; (N2); addn. of Et2NH to soln. of AuCl(CN(Tol-p)) in CH2Cl2; stirring for15 min at room temp.; monitoring by IR; removal of volatiles; washing with n-hexane; crystn. from CH2Cl2/n-hexane; washing with n-hexane; vac.-drying; elem. anal.;
DOI:10.1021/om901026m