C₂₂H₃₆O₃Si

Base Information

Chemical Name:C₂₂H₃₆O₃Si
CAS No.:1454915-84-4
Molecular Formula:C₂₂H₃₆O₃Si
Molecular Weight:376.612
Hs Code.:

C<sub>22</sub>H<sub>36</sub>O<sub>3</sub>Si

Synonyms:C₂₂H₃₆O₃Si

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Chemical Property of C₂₂H₃₆O₃Si

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Technology Process of C₂₂H₃₆O₃Si

There total 8 articles about C₂₂H₃₆O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1454915-83-3
C₁₉H₂₈O₃

: 1454915-84-4
C₂₂H₃₆O₃Si

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc45170d

Reference yield:

: 1454915-72-0
ethyl 2-((1R,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-en-1-yl)acetate

: 1454915-84-4
C₂₂H₃₆O₃Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / -78 - -30 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere

3.2: sat. Na/K tartrate / 2 h / 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

6.1: triethylamine; dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c3cc45170d

Reference yield:

: 1454915-74-2
ethyl 2-((1R,2S,6S)-3-methyl-6-(prop-1-en-2-yl)-2-((trimethylsilyl)oxy)cyclohex-3-en-1-yl) acetate

: 1454915-84-4
C₂₂H₃₆O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere

1.2: sat. Na/K tartrate / 2 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.1: triethylamine; dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

With dmap; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c3cc45170d