2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide

Base Information

Chemical Name:2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide
CAS No.:1447018-14-5
Molecular Formula:C₃₀H₂₃BrF₃N₃O₃S
Molecular Weight:642.496
Hs Code.:

Synonyms:2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide

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Chemical Property of 2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide

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Technology Process of 2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide

There total 4 articles about 2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 714963-55-0
2-(2,4,6-trifluorophenyl)acetyl chloride

: 1447017-93-7
2-amino-N-(3-(benzylthio)-2-(methylcarbamoyl)phenyl)-6-bromobenzamide

: 1447018-14-5
2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1016/j.cclet.2013.04.047

Reference yield:

: 1447017-92-6
2-amino-6-bromo-N-(3-bromo-2-(methylcarbamoyl)phenyl)benzamide

: 1447018-14-5
2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.cclet.2013.04.047

Reference yield:

: 209991-63-9
2,4,6-trifluorophenylacetic acid

: 1447018-14-5
2-(benzylthio)-6-(2-bromo-6-(2-(2,4,6-trifluorophenyl)acetamido)benzamido)-N-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Reflux

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.cclet.2013.04.047