4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one

Base Information

• Chemical Name: 4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one
• CAS No.: 152327-10-1
• Molecular Formula: C₁₇H₂₁F₃O₆S
• Molecular Weight: 410.411

Synonyms:4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one

Chemical Property of 4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one

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Technology Process of 4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one

There total 2 articles about 4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,2-Dimethyl-propionic acid 4-hydroxy-1-((Z)-4-trifluoromethanesulfonyloxy-but-3-enyl)-cyclohexa-2,5-dienylmethyl ester (152377-33-8) → 4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one (152327-10-1)

Guidance literature:

With dipyridinium dichromate; In dichloromethane; at 23 ℃; for 2h;

Reference yield: 71.0%

2,2-Dimethyl-propionic acid 1-((Z)-4-trifluoromethanesulfonyloxy-but-3-enyl)-cyclohexa-2,5-dienylmethyl ester (152327-05-4) → 4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one (152327-10-1)

Guidance literature:

With chromium(VI) oxide; phthalic acid dimethyl ester; In dichloromethane; at -20 - -10 ℃; for 1h;

Reference yield: 61.0%

4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexadien-1-one (152327-10-1) → 2,2-Dimethyl-propionic acid 4-hydroxy-1-((Z)-4-trifluoromethanesulfonyloxy-but-3-enyl)-cyclohexa-2,5-dienylmethyl ester (152377-33-8) + c-4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexen-r-1-ol (152327-06-5)

Guidance literature:

With sodium tetrahydroborate; cerium(III) chloride; In methanol; at -78 ℃; for 1h;

upstream raw materials:

2,2-Dimethyl-propionic acid 1-((Z)-4-trifluoromethanesulfonyloxy-but-3-enyl)-cyclohexa-2,5-dienylmethyl ester

2,2-Dimethyl-propionic acid 4-hydroxy-1-((Z)-4-trifluoromethanesulfonyloxy-but-3-enyl)-cyclohexa-2,5-dienylmethyl ester

Downstream raw materials:

2,2-Dimethyl-propionic acid 4-hydroxy-1-((Z)-4-trifluoromethanesulfonyloxy-but-3-enyl)-cyclohexa-2,5-dienylmethyl ester

c-4-pivaloyloxymethyl-4-((Z)-4-trifluoromethanesulfonyloxy-3-butenyl)-2,5-cyclohexen-r-1-ol

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