fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2]

Base Information

Chemical Name:fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2]
CAS No.:55615-49-1
Molecular Formula:C₂₉H₂₂ClN₂O₃Re
Molecular Weight:668.165
Hs Code.:

Synonyms:fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2]

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Chemical Property of fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2]

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Technology Process of fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2]

There total 1 articles about fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 14099-01-5
rhenium(I) pentacarbonyl chloride

: 5097-93-8
trans-4-styrylpyride

: 55615-49-1
fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2]

Guidance literature:: In toluene; Re-complex and (C6H5)CHCH(C5H4N) refluxed in dry toluene for 12 h; soln. cooled, volume reduced to a min., ppt. filtered under suction, washed with pet spirits (60-80°C);
DOI:10.1021/jp044753+

Reference yield:

: 55615-49-1
fac-[Re(Cl)(CO)3(trans-4-styrylpyridine)2]

: 55658-97-4
Re(CO)3Cl(NC₅H₄CHCHC₆H₅)2

Guidance literature:: With ((C₄H₉)4N)ClO₄; In acetonitrile; Electrolysis; ac electrolysis were carried out under Ar in spectrophotometer cell which were equipped with two platinum foil electrodes connected to Kroencke Model 1246 sine wave generator; 0.1 M (N(CMe3)4)ClO4 as supporting electrolyte; not isolated, monitored by UV at 330 nm;
DOI:10.1021/ja00363a005