C₂₂H₂₄FN₃O

Base Information

Chemical Name:C₂₂H₂₄FN₃O
CAS No.:1383735-28-1
Molecular Formula:C₂₂H₂₄FN₃O
Molecular Weight:365.45
Hs Code.:

C<sub>22</sub>H<sub>24</sub>FN<sub>3</sub>O

Synonyms:C₂₂H₂₄FN₃O

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Chemical Property of C₂₂H₂₄FN₃O

Chemical Property:

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Technology Process of C₂₂H₂₄FN₃O

There total 10 articles about C₂₂H₂₄FN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 405174-97-2
3-bromopicolinaldehyde

: 1383735-28-1
C₂₂H₂₄FN₃O

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium acetate / ethanol; water / 18 h / 50 °C

2.1: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / 1-methyl-pyrrolidin-2-one / 18 h / 120 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 61 h

4.1: acetic anhydride / 28 h / 140 °C / sealed tube

4.2: 6 h / 90 °C

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; water; methanol

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 5 °C

6.2: 16 h / 20 °C

7.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 0.5 h / -78 °C

7.2: 2 h

8.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

8.2: 2 h

9.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / Reflux

9.2: 0.5 h / 0 °C

With lithium aluminium tetrahydride; hydrogen; sodium acetate; acetic anhydride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; lithium diisopropyl amide; copper(l) iodide; palladium 10% on activated carbon; cis-N,N'-dimethyl-1,2-diaminocyclohexane; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1383735-27-0
C₂₂H₂₂FN₃O₂

: 1383735-28-1
C₂₂H₂₄FN₃O

Guidance literature:: C₂₂H₂₂FN₃O₂; With lithium aluminium tetrahydride; In tetrahydrofuran; for 8h; Reflux;

With water; In tetrahydrofuran; at 0 ℃; for 0.5h;

Reference yield:

: (4-fluoro-phenyl)-hydrazine hydrochloride

: 1383735-28-1
C₂₂H₂₄FN₃O

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium acetate / ethanol; water / 18 h / 50 °C

2.1: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / 1-methyl-pyrrolidin-2-one / 18 h / 120 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 61 h

4.1: acetic anhydride / 28 h / 140 °C / sealed tube

4.2: 6 h / 90 °C

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; water; methanol

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 5 °C

6.2: 16 h / 20 °C

7.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 0.5 h / -78 °C

7.2: 2 h

8.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

8.2: 2 h

9.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / Reflux

9.2: 0.5 h / 0 °C

With lithium aluminium tetrahydride; hydrogen; sodium acetate; acetic anhydride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; lithium diisopropyl amide; copper(l) iodide; palladium 10% on activated carbon; cis-N,N'-dimethyl-1,2-diaminocyclohexane; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;