1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene

Base Information

• Chemical Name: 1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene
• CAS No.: 1133728-88-7
• Molecular Formula: C₂₅H₂₄O₃
• Molecular Weight: 372.464
• Mol file: 1133728-88-7.mol

Synonyms:1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene

Chemical Property of 1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene

Chemical Property:

Purity/Quality:

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Technology Process of 1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene

There total 1 articles about 1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-allyl-3,5-bis (benzyloxy)phenol (1133728-87-6) + ethylene dibromide (106-93-4) → 1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene (1133728-88-7)

Guidance literature:

2-allyl-3,5-bis (benzyloxy)phenol; ethylene dibromide; With potassium carbonate; In acetone; at 60 ℃; for 38h;

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; benzene; for 1h;

DOI:10.1016/j.tetlet.2009.01.017

Reference yield:

1-((4-allyl-3-(benzyloxy)-5-(vinyloxy)phenoxy)methyl)benzene (1133728-88-7) → 5,7-bis(benzyloxy)-4H-chromene (1133728-90-1)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 60 ℃; for 0.166667h;

DOI:10.1016/j.tetlet.2009.01.017

upstream raw materials:

2-allyl-3,5-bis (benzyloxy)phenol

ethylene dibromide

Downstream raw materials:

5,7-bis(benzyloxy)-4H-chromene