1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane

Base Information

Chemical Name:1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane
CAS No.:125682-97-5
Molecular Formula:C₄₁H₄₉N₅O₁₂S₅
Molecular Weight:964.196
Hs Code.:

Synonyms:1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane

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Chemical Property of 1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane

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Technology Process of 1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane

There total 3 articles about 1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 124-63-0
methanesulfonyl chloride

: 125682-96-4
1,9-bis<6-(hydroxymethyl)pyridin-2-yl>-2,5,8-tritosyl-2,5,8-triazanonane

: 125682-97-5
1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane

Guidance literature:: With ethyl azide; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1002/hlca.19890720525

Reference yield:

: 56187-04-3
1,4,7-tritosyl-1,4,7-triazaheptane

: 125682-97-5
1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane

Guidance literature:: Multi-step reaction with 3 steps

1: Na / 2 h / Heating

2: 54 percent / dimethylformamide / 5 h / 90 °C

3: 93 percent / EtN₃ / CH₂Cl₂ / 3 h / Ambient temperature

With sodium; ethyl azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19890720525

Reference yield:

: 52601-80-6
N,N’,N”-tris(p-toluenesulfonyl)diethylenetriamine N,N-disodium salt

: 125682-97-5
1,9-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,5,8-tritosyl-2,5,8-triazanonane

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / dimethylformamide / 5 h / 90 °C

2: 93 percent / EtN₃ / CH₂Cl₂ / 3 h / Ambient temperature

With ethyl azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19890720525