N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

Base Information

Chemical Name:N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride
CAS No.:1370443-50-7
Molecular Formula:C₃₃H₄₀N₆O₅
Molecular Weight:600.718
Hs Code.:

N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

Synonyms:N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

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Chemical Property of N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

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Technology Process of N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

There total 7 articles about N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1187583-52-3
C₁₁H₁₈N₂O

: 83204-68-6
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride

: 108-00-9
N,N-dimethylethylenediamine

: 1370443-50-7
N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

: 1370443-51-8
N,N′-bis-((dimethylamino)ethylamino)-2-bromo-6-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

Guidance literature:: 2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride; N,N-dimethylethylenediamine; With acetic acid; at 130 ℃; for 0.5h;

C₁₁H₁₈N₂O; In N,N-dimethyl-formamide; at 180 ℃; for 0.05h; under 12929 Torr; Microwave irradiation;
DOI:10.1039/c2ob06816h

Reference yield: 25.0%

: 1187583-52-3
C₁₁H₁₈N₂O

: 83204-68-6
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride

: 108-00-9
N,N-dimethylethylenediamine

: 1370443-50-7
N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

: 1370443-51-8
N,N′-bis-((dimethylamino)ethylamino)-2-bromo-6-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

: N,N′-bis-((dimethylamino)ethylamino)-2,6-bis(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide tetrahydrochloride

Guidance literature:: 2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride; N,N-dimethylethylenediamine; With acetic acid; at 130 ℃; for 0.5h;

C₁₁H₁₈N₂O; In N,N-dimethyl-formamide; at 180 ℃; for 0.0833333h; under 12929 Torr; Microwave irradiation;
DOI:10.1039/c2ob06816h

Reference yield:

: 51-67-2
tyrosamine

: 1370443-50-7
N,N′-bis-((dimethylamino)ethylamino)-2-(2-(3-(dimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4-5,8-naphthalenetetracarboxylic bisimide trihydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 2 h / 20 °C

2.1: ethanol / 2 h / Inert atmosphere; Reflux

3.1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4.1: acetic acid / 0.5 h / 130 °C

4.2: 0.05 h / 180 °C / 12929 Torr / Microwave irradiation

With triethylsilane; acetic acid; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/c2ob06816h