3,7-bis(dibutylamino)-3H,7H-1λ4,5λ4,2,4,6,8,3,7-dithiatetrazadiborocine

Base Information

Chemical Name:3,7-bis(dibutylamino)-3H,7H-1λ4,5λ4,2,4,6,8,3,7-dithiatetrazadiborocine
CAS No.:154108-70-0
Molecular Formula:C₁₆H₃₆B₂N₆S₂
Molecular Weight:398.256
Hs Code.:

Synonyms:3,7-bis(dibutylamino)-3H,7H-1λ4,5λ4,2,4,6,8,3,7-dithiatetrazadiborocine

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Chemical Property of 3,7-bis(dibutylamino)-3H,7H-1λ4,5λ4,2,4,6,8,3,7-dithiatetrazadiborocine

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Technology Process of 3,7-bis(dibutylamino)-3H,7H-1λ4,5λ4,2,4,6,8,3,7-dithiatetrazadiborocine

There total 1 articles about 3,7-bis(dibutylamino)-3H,7H-1λ4,5λ4,2,4,6,8,3,7-dithiatetrazadiborocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 503027-47-2,503027-48-3,155139-78-9,18156-25-7
N,N'-bis(trimethylsilyl)sulfurdiimide

: 18379-71-0
Cl₂BN(n-C₄H₉)2

: 75-77-4
chloro-trimethyl-silane

: 154108-70-0
3,7-bis(dibutylamino)-3H,7H-1λ4,5λ4,2,4,6,8,3,7-dithiatetrazadiborocine

Guidance literature:: In pentane; under N2, dropwise addn. within 2 h of borane in pentane at 0°C to a stirred soln. of diimide in pentane, stirred overnight; removal of volatiles in vac., taken up in pentane, filtered, removal of solvent in vac.; elem. anal.;