1-[(4-chlorophenyl)sulfanyl]ethenyl dimethyl phosphate

Base Information

• Chemical Name: 1-[(4-chlorophenyl)sulfanyl]ethenyl dimethyl phosphate
• CAS No.: 2595-53-1
• Molecular Formula: C₁₀H₁₂ClO₄PS
• Molecular Weight: 294.696
• Mol file: 2595-53-1.mol

Synonyms:Phosphoricacid, 1-[(p-chlorophenyl)thio]vinyl dimethyl ester (7CI,8CI); Ketene,S-p-chlorophenyl monothiohemiacetal, dimethyl phosphate; SD 7587; Shell SD 7587

Chemical Property of 1-[(4-chlorophenyl)sulfanyl]ethenyl dimethyl phosphate

Chemical Property:

• Vapor Pressure: 6.04E-05mmHg at 25°C
• Boiling Point: 356.3°C at 760 mmHg
• Flash Point: 169.3°C
• Density: 1.33g/cm³

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[(4-chlorophenyl)sulfanyl]ethenyl dimethyl phosphate

There total 1 articles about 1-[(4-chlorophenyl)sulfanyl]ethenyl dimethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-thioacetic acid S-(4-chloro-phenyl ester) (24197-67-9) + phosphorous acid trimethyl ester (121-45-9) → 1-(p-Chlor-phenylmercapto)-vinyl-dimethylphosphat (2595-53-1)

Guidance literature:

DOI:10.1021/jo01276a037

Reference yield:

1-(p-Chlor-phenylmercapto)-vinyl-dimethylphosphat (2595-53-1) → 1-(p-Chlor-phenylsulfin)-vinyl-dimethylphosphat (17604-58-9)

Guidance literature:

With peracetic acid; In chloroform;

DOI:10.1021/jo01276a037

Reference yield:

1-(p-Chlor-phenylmercapto)-vinyl-dimethylphosphat (2595-53-1) → 1-(p-Chlor-phenylsulfon)-vinyl-dimethylphosphat (17604-62-5)

Guidance literature:

With monoperoxyphthalic acid; In diethyl ether;

DOI:10.1021/jo01276a037

upstream raw materials:

chloro-thioacetic acid S-(4-chloro-phenyl ester)

phosphorous acid trimethyl ester

Downstream raw materials:

1-(p-Chlor-phenylsulfin)-vinyl-dimethylphosphat

1-(p-Chlor-phenylsulfon)-vinyl-dimethylphosphat

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