Technology Process of C26H33NO4
There total 7 articles about C26H33NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
DOI:10.1021/ja00281a047
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) NaBH4 / 1.) MeOH, 0 deg C, 10 min; 2.) 3 h, r.t.
2: 1.) 3N NaOH; 2.) NaH, 18-crown-6 / 1.) MeOH, r.t; 2.) THF, DMF
3: 1.) 8percent KOH / 1.) EtOH, reflux
4: Et3N, (COCl)2 / dimethylsulfoxide
5: 79.2 percent / t-BuOK / diethyl ether / 2 h / -25 °C
6: 1.) BF3*Et2O; 2.) Jones reagent / 1.) toluene, -15 deg C, 0.5 h; 2.) acetone, 0 deg C, 5 min
7: LiALH4 / tetrahydrofuran
With
potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; jones reagent; oxalyl dichloride; 18-crown-6 ether; boron trifluoride diethyl etherate; potassium tert-butylate; sodium hydride; triethylamine;
In
tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1021/ja00281a047
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) 3N NaOH; 2.) NaH, 18-crown-6 / 1.) MeOH, r.t; 2.) THF, DMF
2: 1.) 8percent KOH / 1.) EtOH, reflux
3: Et3N, (COCl)2 / dimethylsulfoxide
4: 79.2 percent / t-BuOK / diethyl ether / 2 h / -25 °C
5: 1.) BF3*Et2O; 2.) Jones reagent / 1.) toluene, -15 deg C, 0.5 h; 2.) acetone, 0 deg C, 5 min
6: LiALH4 / tetrahydrofuran
With
potassium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; jones reagent; oxalyl dichloride; 18-crown-6 ether; boron trifluoride diethyl etherate; potassium tert-butylate; sodium hydride; triethylamine;
In
tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1021/ja00281a047
