tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate

Base Information

Chemical Name:tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate
CAS No.:1092938-87-8
Molecular Formula:C₂₃H₃₀N₄O₂
Molecular Weight:394.517
Hs Code.:

Synonyms:tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate

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Technology Process of tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate

There total 1 articles about tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 713529-91-0
4-(2,6-dimethyl-benzylamino)-1,2-dimethyl-1H-benzimidazole-6-carboxylic acid

: 75-65-0
tert-butyl alcohol

: 1092938-87-8
tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate

Guidance literature:: With diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine; for 1.5h; Heating / reflux;

Reference yield: 88.0%

: 1092938-87-8
tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate

: 1092938-88-9
N₄-(2,6-dimethylbenzyl)-1,2-trimethyl-1H-benzimidazole-4,6-diamine

Guidance literature:: With hydrogenchloride; In methanol; at 45 ℃;

Reference yield:

: 1092938-87-8
tert-butyl {4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}carbamate

: 1092938-44-7
N-{4-[(2,6-dimethylbenzyl)amino]-1,2-dimethyl-1H-benzimidazol-6-yl}-N-methylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / methanol / 45 °C

2.1: sodium methylate / methanol / 1 h / Heating / reflux

2.2: 1 h / Heating / reflux

3.1: dmap / dichloromethane / 2 h / 20 °C

With hydrogenchloride; dmap; sodium methylate; In methanol; dichloromethane;