5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

Base Information

Chemical Name:5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl
CAS No.:1256724-00-1
Molecular Formula:C₄₄H₅₈O₆
Molecular Weight:682.941
Hs Code.:

Synonyms:5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

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Chemical Property of 5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

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Technology Process of 5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

There total 1 articles about 5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₅₈O₈

: 1256724-00-1
5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

Guidance literature:: With triethylsilane; trifluoroacetic acid; at 20 - 75 ℃; for 19h;
DOI:10.1021/jm100746q

Reference yield: 80.0%

: 1256724-00-1
5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

: 1256724-24-9
5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

Guidance literature:: 5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl; With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 3h;

With hydrogenchloride; In dichloromethane; water; at 20 ℃;
DOI:10.1021/jm100746q

Reference yield:

: 1256724-00-1
5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

: 1256724-05-6
5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane / 3 h / -78 - 20 °C

1.2: 20 °C

2.1: iron(III) chloride; acetic acid / water; acetone / 60 - 67 °C

With iron(III) chloride; boron tribromide; acetic acid; In dichloromethane; water; acetone;
DOI:10.1021/jm100746q