5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

Base Information

Chemical Name:5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol
CAS No.:1256724-24-9
Molecular Formula:C₃₈H₄₆O₆
Molecular Weight:598.78
Hs Code.:

Synonyms:5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

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Chemical Property of 5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

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Technology Process of 5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

There total 2 articles about 5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1256724-00-1
5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

: 1256724-24-9
5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

Guidance literature:: 5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl; With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 3h;

With hydrogenchloride; In dichloromethane; water; at 20 ℃;
DOI:10.1021/jm100746q

Reference yield:

: C₄₄H₅₈O₈

: 1256724-24-9
5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylsilane; trifluoroacetic acid / 19 h / 20 - 75 °C

2.1: boron tribromide / dichloromethane / 3 h / -78 - 20 °C

2.2: 20 °C

With triethylsilane; boron tribromide; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm100746q

Reference yield: 50.0%

: 1256724-24-9
5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

: 1256724-05-6
5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

Guidance literature:: 5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol; With iron(III) chloride; acetic acid; In water; acetone; at 60 - 67 ℃;

With sulfuric acid; In water; acetone;
DOI:10.1021/jm100746q