5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

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Chemical Name:5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone
CAS No.:1256724-05-6
Molecular Formula:C₃₈H₄₂O₈
Molecular Weight:626.747
Hs Code.:

Synonyms:5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

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Chemical Property of 5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

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Technology Process of 5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

There total 3 articles about 5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1256724-24-9
5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol

: 1256724-05-6
5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

Guidance literature:: 5,5'-bis(2-cyclohexylethyl)-3,3'-dimethyl-2,2'-binaphthyl-1,1',6,6',7,7'-hexaol; With iron(III) chloride; acetic acid; In water; acetone; at 60 - 67 ℃;

With sulfuric acid; In water; acetone;
DOI:10.1021/jm100746q

Reference yield:

: C₄₄H₅₈O₈

: 1256724-05-6
5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylsilane; trifluoroacetic acid / 19 h / 20 - 75 °C

2.1: boron tribromide / dichloromethane / 3 h / -78 - 20 °C

2.2: 20 °C

3.1: iron(III) chloride; acetic acid / water; acetone / 60 - 67 °C

With triethylsilane; iron(III) chloride; boron tribromide; acetic acid; trifluoroacetic acid; In dichloromethane; water; acetone;
DOI:10.1021/jm100746q

Reference yield:

: 1256724-00-1
5,5'-bis(2-cyclohexylethyl)-1,1',6,6',7,7'-hexamethoxy-3,3'-dimethyl-2,2'-binaphthyl

: 1256724-05-6
5,5'-bis(2-cyclohexylethyl)-6,6',7,7'-tetrahydroxy-3,3'-dimethyl-2,2'-binaphthyl-1,1',4,4'-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane / 3 h / -78 - 20 °C

1.2: 20 °C

2.1: iron(III) chloride; acetic acid / water; acetone / 60 - 67 °C

With iron(III) chloride; boron tribromide; acetic acid; In dichloromethane; water; acetone;
DOI:10.1021/jm100746q