2-Chloro-N-[(dimethylamino)methylene]-4-fluorobenzenesulfonamide

Base Information

Chemical Name:2-Chloro-N-[(dimethylamino)methylene]-4-fluorobenzenesulfonamide
CAS No.:69156-31-6
Molecular Formula:C₉H₁₀ClFN₂O₂S
Molecular Weight:264.708
Hs Code.:
DSSTox Substance ID:DTXSID901170431

Synonyms:DTXSID901170431;2-Chloro-N-[(dimethylamino)methylene]-4-fluorobenzenesulfonamide;69156-31-6

Suppliers and Price of 2-Chloro-N-[(dimethylamino)methylene]-4-fluorobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Chloro-N-[(dimethylamino)methylene]-4-fluorobenzenesulfonamide

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:264.0135546
Heavy Atom Count:16
Complexity:353

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)C=NS(=O)(=O)C1=C(C=C(C=C1)F)Cl

Technology Process of 2-Chloro-N-[(dimethylamino)methylene]-4-fluorobenzenesulfonamide

There total 4 articles about 2-Chloro-N-[(dimethylamino)methylene]-4-fluorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 69156-30-5
2-chloro-4-fluorobenzenesulfonamide

: 69156-31-6
C₉H₁₀ClFN₂O₂S

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; for 30h;
DOI:10.1021/jm00362a017

Reference yield:

: 2106-02-7
2-chloro-4-fluoroaniline

: 69156-31-6
C₉H₁₀ClFN₂O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, HCl, 2.) CuCl₂*2H₂O, HOAc, SO₂ / 1.) H₂O, 2.) H₂O, RT

2: 90 percent / NH₃ / Ambient temperature

3: 87 percent / dimethylformamide / 30 h / 60 °C

With hydrogenchloride; sulfur dioxide; ammonia; acetic acid; sodium nitrite; In N,N-dimethyl-formamide;
DOI:10.1021/jm00362a017

Reference yield:

: 85958-57-2
2-chloro-4-fluorobenzene-1-sulfonyl chloride

: 69156-31-6
C₉H₁₀ClFN₂O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NH₃ / Ambient temperature

2: 87 percent / dimethylformamide / 30 h / 60 °C

With ammonia; In N,N-dimethyl-formamide;
DOI:10.1021/jm00362a017