2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

Base Information

Chemical Name:2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane
CAS No.:126750-14-9
Molecular Formula:C₂₆H₃₆O₇
Molecular Weight:460.568
Hs Code.:

Synonyms:2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

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Chemical Property of 2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

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Technology Process of 2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

There total 6 articles about 2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 126750-09-2
3-(p-ethoxyethoxyethoxyphenyl)-2,4-dihydroxymethylpentane-1,5-diol

: 100-52-7
benzaldehyde

: 126750-14-9
2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

Guidance literature:: With hydrogenchloride; In N,N-dimethyl-formamide; at 30 ℃; for 7h;

Reference yield:

: 126750-26-3
1-ethoxy-2-(2-(2-iodoethoxy)ethoxy)ethane

: 126750-14-9
2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium hydroxide / 1.) butyl alcolhol, reflux, 1 h, 2.) reflux, 12 h

2: 78 percent / piperidine / benzene / 12 h / Heating

3: 63 percent / activated zinc, iodine / tetrahydrofuran / 5 h / 50 °C

4: 85 percent / lithium aluminum hydride / diethyl ether / 1.) reflux, 2 h, 2.) room temp., 24 h

5: 70 percent / conc. HCl / dimethylformamide / 7 h / 30 °C

With piperidine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; iodine; zinc; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; benzene;

Reference yield:

: 117420-31-2
4-(2-(2-ethoxyethoxy)ethoxy)benzaldehyde

: 126750-14-9
2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / piperidine / benzene / 12 h / Heating

2: 63 percent / activated zinc, iodine / tetrahydrofuran / 5 h / 50 °C

3: 85 percent / lithium aluminum hydride / diethyl ether / 1.) reflux, 2 h, 2.) room temp., 24 h

4: 70 percent / conc. HCl / dimethylformamide / 7 h / 30 °C

With piperidine; hydrogenchloride; lithium aluminium tetrahydride; iodine; zinc; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; benzene;