(+/-)-(Z)-9-methylchorismic acid

Base Information

Chemical Name:(+/-)-(Z)-9-methylchorismic acid
CAS No.:116130-11-1
Molecular Formula:C₁₁H₁₂O₆
Molecular Weight:240.213
Hs Code.:

Synonyms:(+/-)-(Z)-9-methylchorismic acid

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Chemical Property of (+/-)-(Z)-9-methylchorismic acid

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Technology Process of (+/-)-(Z)-9-methylchorismic acid

There total 2 articles about (+/-)-(Z)-9-methylchorismic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 116130-16-6
(+/-)-(Z)-(3β,4α,5β)-3-<(1-carboxypropenyl)oxy>-4-hydroxy-5-(phenylseleno)-1-cyclohexene-1-carboxylic acid

: 116130-11-1
(+/-)-(Z)-9-methylchorismic acid

Guidance literature:: With dihydrogen peroxide; In acetone; at 0 ℃; for 1h;
DOI:10.1021/jo00256a016

Reference yield:

: 116130-11-1,116183-36-9,116257-37-5
(-)-9-methylchorismic acid

: 116130-11-1,116183-36-9,116257-37-5
(-)-(E)-9-methylchorismic acid

: 116257-37-5
(-)-(Z)-9-methylchorismic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 0 ℃; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00256a016

Reference yield: 34.0%

: 116130-11-1
(+/-)-(Z)-9-methylchorismic acid

: 600-18-0
2-Oxobutyric acid

: 4658-69-9
α-keto-β-phenylbutyric acid

: 116130-27-9
1-(2-Carboxy-1-methyl-2-oxo-ethyl)-4-hydroxy-cyclohexa-2,5-dienecarboxylic acid

: 99-96-7
4-hydroxy-benzoic acid

Guidance literature:: In water-d2; at 30 ℃; Product distribution; Rate constant; uncatalysed and nish chorismate mutase catalyst;
DOI:10.1021/jo00256a016