4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Chemical Name:4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside
CAS No.:862851-26-1
Molecular Formula:C₂₃H₂₆O₅S
Molecular Weight:414.522
Hs Code.:

Synonyms:4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Chemical Property of 4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Technology Process of 4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

There total 4 articles about 4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 116-11-0
2-Methoxypropene

: 219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 862851-26-1
4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With (1S)-10-camphorsulfonic acid; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1021/ol051178z

Reference yield:

: 77-76-9
2,2-dimethoxy-propane

: 219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 862851-26-1
4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: vanadyl triflate; In acetonitrile; at 20 ℃; for 20h;
DOI:10.1016/j.carres.2006.04.001

Reference yield:

: 1152-39-2
p-methylphenyl 1-thio-β-D-glucopyranoside

: 862851-26-1
4-methylphenyl 2,3-di-O-isoporpylidene-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / VO(OTf)2*xH₂O / acetonitrile / 8 h / 20 °C

2: 94 percent / D-camphorsulfonic acid / tetrahydrofuran / 1.5 h / 20 °C

With vanadyl triflate; (1S)-10-camphorsulfonic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol051178z