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Technology Process of [((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]

[((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]

Base Information
  • Chemical Name:[((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]
  • CAS No.:36499-78-2
  • Molecular Formula:C7CrF3O7*C36H30NP2
  • Molecular Weight:843.652
  • Hs Code.:
[((C<sub>6</sub>H<sub>5</sub>)3P)2N]<sup>(1+)</sup>*[Cr(CO)5OOCCF<sub>3</sub>]<sup>(1-)</sup>=[((C<sub>6</sub>H<sub>5</sub>)3P)2N][Cr(CO)5OOCCF<sub>3</sub>]

Synonyms:[((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]

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Chemical Property of [((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]
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Technology Process of [((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]

There total 3 articles about [((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}
65650-76-2

bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}

silver trifluoroacetate
2966-50-9

silver trifluoroacetate

[((C<sub>6</sub>H<sub>5</sub>)3P)2N]<sup>(1+)</sup>*[Cr(CO)5OOCCF<sub>3</sub>]<sup>(1-)</sup>=[((C<sub>6</sub>H<sub>5</sub>)3P)2N][Cr(CO)5OOCCF<sub>3</sub>]
36499-78-2

[((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]

Guidance literature:
In dichloromethane; byproducts: AgCl; 10 min; filtered under N2, evapd. in vac., recrystd. from THF/hexane at -10°C;
DOI:10.1021/ja00392a026

Reference yield:

bis(triphenylphosphine)iminium chloride
21050-13-5

bis(triphenylphosphine)iminium chloride

[((C<sub>6</sub>H<sub>5</sub>)3P)2N]<sup>(1+)</sup>*[Cr(CO)5OOCCF<sub>3</sub>]<sup>(1-)</sup>=[((C<sub>6</sub>H<sub>5</sub>)3P)2N][Cr(CO)5OOCCF<sub>3</sub>]
36499-78-2

[((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]

Guidance literature:
Multi-step reaction with 2 steps
1: diethylene glycol dimethyl ether
2: dichloromethane
In dichloromethane; diethylene glycol dimethyl ether;
DOI:10.1021/ja00392a026

Reference yield:

chromium<sup>(0)</sup> hexacarbonyl
199620-14-9,13007-92-6

chromium(0) hexacarbonyl

[((C<sub>6</sub>H<sub>5</sub>)3P)2N]<sup>(1+)</sup>*[Cr(CO)5OOCCF<sub>3</sub>]<sup>(1-)</sup>=[((C<sub>6</sub>H<sub>5</sub>)3P)2N][Cr(CO)5OOCCF<sub>3</sub>]
36499-78-2

[((C6H5)3P)2N](1+)*[Cr(CO)5OOCCF3](1-)=[((C6H5)3P)2N][Cr(CO)5OOCCF3]

Guidance literature:
Multi-step reaction with 2 steps
1: diethylene glycol dimethyl ether
2: dichloromethane
In dichloromethane; diethylene glycol dimethyl ether;
DOI:10.1021/ja00392a026
upstream raw materials:

bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}

silver trifluoroacetate

bis(triphenylphosphine)iminium chloride

chromium(0) hexacarbonyl

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