bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}

Base Information

• Chemical Name: bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}
• CAS No.: 65650-76-2
• Molecular Formula: C₅ClCrO₅*C₃₆H₃₀NP₂
• Molecular Weight: 766.089

Synonyms:bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}

Chemical Property of bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of bis(triphenylphosphine)nitrogen{Cr(CO)5Cl}

There total 14 articles about bis(triphenylphosphine)nitrogen{Cr(CO)5Cl} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

{PPN}{HCr(CO)5} (78362-94-4) + 4-bromobutyroyl chloride (927-58-2) → 4-bromobutyraldehyde (38694-47-2) + bis(triphenylphosphine)nitrogen{Cr(CO)5Cl} (65650-76-2)

Guidance literature:

In tetrahydrofuran; 1:1 molar ratio; THF, 25°C;; detected by NMR and IR spectra; and GC analysis,;

Reference yield: 95.0%

{PPN}{HCr(CO)5} (78362-94-4) + n-valeryl chloride (638-29-9) → pentanal (110-62-3) + bis(triphenylphosphine)nitrogen{Cr(CO)5Cl} (65650-76-2)

Guidance literature:

In tetrahydrofuran; 1:1 molar ratio, THF, 25°C;; detected by NMR and IR spectra; and GC analysis,;

Reference yield: 95.0%

{PPN}{HCr(CO)5} (78362-94-4) + deuteromethanol (1455-13-6) + n-valeryl chloride (638-29-9) → bis(triphenylphosphine)nitrogen{Cr(CO)5Cl} (65650-76-2) + [1-(2)H1]-pentanal (35667-35-7)

Guidance literature:

In tetrahydrofuran; 1:1 molar ratio, THF, 25°C;; detected by NMR and IR spectra; and GC analysis,;

upstream raw materials:

pentacarbonyl(thiocarbonyl)chromium⁽⁰⁾

bis(triphenylphosphine)iminium chloride

chromium⁽⁰⁾ hexacarbonyl

{PPN}{HCr(CO)5}

Downstream raw materials:

Cr(CO)5SH^(1-)*(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾={Cr(CO)5SH}(C₆H₅)3PNP(C₆H₅)3

[Bis(triphenylphosphan)nitrogenium]-pentacarbonyl(hydrogentellurido)chromat⁽⁰⁾

[Bis(triphenylphosphan)nitrogenium]-pentacarbonyl(hydrogenselenido)chromat⁽⁰⁾

[((C₆H₅)3P)2N]⁽¹⁺⁾*[Cr(CO)5OOCCF₃]^(1-)=[((C₆H₅)3P)2N][Cr(CO)5OOCCF₃]

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