2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid

Base Information

Chemical Name:2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid
CAS No.:120229-81-4
Molecular Formula:C₂₆H₂₉NO₃
Molecular Weight:403.521
Hs Code.:

Synonyms:2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid

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Chemical Property of 2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid

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Technology Process of 2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid

There total 3 articles about 2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 120229-68-7
5,6,7,8-Tetrahydro-7,7-dimethyl-2-(methylphenylamino)-3-phenylspiro-<4H-chromen-4,1'-cyclopropan>-5-on

: 120262-50-2
5,6,7,8-Tetrahydro-7,7-dimethyl-3-phenylspiro-2,5-dion

: 120229-81-4
2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid

Guidance literature:: With sodium hydrogen sulfate; In dichloromethane; at 50 ℃; for 216h;

Reference yield:

: 110174-72-6
2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate

: 120229-81-4
2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid

Guidance literature:: Multi-step reaction with 2 steps

1: 2) 1,2-diaminoethan / acetone; ethanol / 1) CH₂Cl₂, 4 h, reflux, 2) H₂O

2: 79 percent / 1M aq. NaHSO₄ / CH₂Cl₂ / 216 h / 50 °C

With sodium hydrogen sulfate; ethylenediamine; In ethanol; dichloromethane; acetone;

Reference yield:

: 110174-70-4
5,5-Dimethyl-2-<1-(1-piperidinio)-cyclopropyl>-1-oxo-2-cyclohexen-3-olat

: 120229-81-4
2-<1-(2-Hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-N-methyl-N,2-diphenylacetamid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / ethyldiisopropylamine / CH₂Cl₂

2: 2) 1,2-diaminoethan / acetone; ethanol / 1) CH₂Cl₂, 4 h, reflux, 2) H₂O

3: 79 percent / 1M aq. NaHSO₄ / CH₂Cl₂ / 216 h / 50 °C

With sodium hydrogen sulfate; ethylenediamine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; acetone;