5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine

Base Information

• Chemical Name: 5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine
• CAS No.: 1198476-36-6
• Molecular Formula: C₁₇H₂₆N₂Si
• Molecular Weight: 286.492

Synonyms:5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine

Chemical Property of 5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine

Chemical Property:

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Technology Process of 5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine

There total 1 articles about 5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

chloro-trimethyl-silane (75-77-4) + bromobenzene (108-86-1,52753-63-6) + 2,2,3,3-tetramethylsuccinonitrile (3333-52-6) → 5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine (1198476-36-6)

Guidance literature:

bromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

2,2,3,3-tetramethylsuccinonitrile; In tetrahydrofuran; hexane; at -78 - 0 ℃; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.200901187

Reference yield: 26.0%

5-phenyl-3,3,4,4-tetramethyl-N-(trimethylsilyl)-3,4-dihydropyrrol-2-imine (1198476-36-6) → 2,2,3,3,7,7,8,8,12,12,13,13,17,17,18,18-hexadecamethyl-1,6,11,16-tetraphenyl-1,2,3,6,7,8,10,11,12,13,16,17,18,20-tetradecahydro-porphyrazin

Guidance literature:

In dichloromethane;

DOI:10.1002/chem.200901187

upstream raw materials:

chloro-trimethyl-silane

bromobenzene

2,2,3,3-tetramethylsuccinonitrile

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