[4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: [4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester
• CAS No.: 913094-50-5
• Molecular Formula: C₂₀H₃₁N₃O₆
• Molecular Weight: 409.483

Synonyms:[4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester

Chemical Property of [4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester

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Technology Process of [4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester

There total 2 articles about [4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Z-Orn(Boc)-OH (7733-29-1,199924-46-4) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → [4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester (913094-50-5)

Guidance literature:

Z-Orn(Boc)-OH; N,O-dimethylhydroxylamine*hydrochloride; With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield: 93.0%

Nα-(benzyloxycarbonyl)-Nδ-(tert-butoxycarbonyl)-L-ornithine methyl ester (32393-52-5) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → [4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester (913094-50-5)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 18h;

DOI:10.1021/ol061736p

Reference yield: 99.0%

[4-benzyloxycarbonylamino-4-(methoxy-methyl-carbamoyl)-butyl]-carbamic acid tert-butyl ester (913094-50-5) → C15H23N3O4 (1224923-53-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.bmcl.2010.01.099

upstream raw materials:

N^α-(benzyloxycarbonyl)-N^δ-(tert-butoxycarbonyl)-L-ornithine methyl ester

N,O-dimethylhydroxylamine*hydrochloride

Z-Orn(Boc)-OH

Downstream raw materials:

(5S)-5-benzyloxycarbonylamino-8-tert-butyloxycarbonylamino-4-oxo-1-octene

(1S,10S)-1-benzyloxycarbonylamino-7,8-didehydroquinolizidine

((2S,3S)-1,2-Diallyl-piperidin-3-yl)-carbamic acid benzyl ester

Methanesulfonic acid (1R,2S)-1-allyl-5-amino-2-benzyloxycarbonylamino-pentyl ester

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