N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide

Base Information

Chemical Name:N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide
CAS No.:1569642-93-8
Molecular Formula:C₃₆H₃₀Cl₂N₆O₈
Molecular Weight:745.576
Hs Code.:

Synonyms:N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide

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Technology Process of N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide

There total 3 articles about N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 79-37-8
oxalyl dichloride

: 1569642-73-4
3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbohydrazide

: 1569642-93-8
N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1016/j.bmc.2014.01.025

Reference yield:

: 151290-21-0
3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole

: 1569642-93-8
N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-dichloro-ethane / 3 h / Reflux

2: hydrazine hydrate; triethylamine / acetonitrile / 1 h / 20 °C

3: triethylamine / dichloromethane / 1.5 h / 20 °C

With hydrazine hydrate; triethylamine; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.bmc.2014.01.025

Reference yield:

: 3-(4-chlorophenyl)-4,6-dimethoxy-7-trichloroacetyl-1H-indole

: 1569642-93-8
N,N'-bis(3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbonyl)oxalohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate; triethylamine / acetonitrile / 1 h / 20 °C

2: triethylamine / dichloromethane / 1.5 h / 20 °C

With hydrazine hydrate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2014.01.025