((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

Base Information

Chemical Name:((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br
CAS No.:1164223-66-8
Molecular Formula:C₆₇H₆₉BrN₂O₄
Molecular Weight:1046.2
Hs Code.:

((CH<sub>3</sub>)3CC<sub>6</sub>H<sub>4</sub>)3CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>CH<sub>2</sub>O)3C<sub>6</sub>H<sub>4</sub>C<sub>12</sub>H<sub>6</sub>N<sub>2</sub>C<sub>6</sub>H<sub>4</sub>Br

Synonyms:((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

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Chemical Property of ((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

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Technology Process of ((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

There total 9 articles about ((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1164223-63-5
2-(4-hydroxyphenyl)-9-(4-bromophenyl)-1,10-phenanthroline

: 1164223-56-6
2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide

: 1164223-66-8
((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1002/anie.200903311

Reference yield:

: 1208256-41-0
C₄₄H₅₈O₆S

: 1164223-66-8
((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 16 h / Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C

With caesium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetone; 2: Williamson synthesis;
DOI:10.1039/b9nj00296k

Reference yield:

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 1164223-66-8
((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / N,N-dimethyl-formamide / 90 h / 48 °C

2: triethylamine / dichloromethane / 4 h / 0 °C

3: sodium iodide / acetone / 16 h / Inert atmosphere

4: caesium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C

With caesium carbonate; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone; 4: Williamson synthesis;
DOI:10.1039/b9nj00296k