2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide

Base Information

• Chemical Name: 2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide
• CAS No.: 1164223-56-6
• Molecular Formula: C₄₃H₅₅IO₃
• Molecular Weight: 746.812
• Mol file: 1164223-56-6.mol

Synonyms:2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide

Chemical Property of 2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide

There total 6 articles about 2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide (1596368-20-5) → 2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide (1164223-56-6)

Guidance literature:

With sodium iodide; In acetone; for 72h; Reflux; Inert atmosphere;

DOI:10.1021/ja5013596

Reference yield: 95.0%

C44H58O6S (1208256-41-0) → 2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide (1164223-56-6)

Guidance literature:

With sodium iodide; In acetone; for 16h; Reflux; Inert atmosphere;

DOI:10.1002/chem.200802510

Reference yield:

2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol (351523-94-9) → 2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide (1164223-56-6)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 0 °C

2: sodium iodide / acetone / 16 h / Inert atmosphere

With triethylamine; sodium iodide; In dichloromethane; acetone;

DOI:10.1039/b9nj00296k

upstream raw materials:

C₄₄H₅₈O₆S

2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol

2-[2-(chloroethoxy)ethoxy]ethanol

4-[tris-(4-tert-butylphenyl)methyl]phenol

Downstream raw materials:

((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄B(neopentyl glycolato)