Technology Process of C32H35N3O6
There total 9 articles about C32H35N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C8H15N3; 5,6-bis((4-methoxybenzyl)oxy)isobenzofuran-1,3-dione;
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 4h;
Inert atmosphere;
With
sodium cyanoborohydride; acetic acid;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: water; toluene; methanol / 20 °C / Inert atmosphere
2.1: methanol; hydrogenchloride / 1,4-dioxane / 4 h / 0 - 20 °C / Inert atmosphere
3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; methanol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
1,4-dioxane; methanol; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol; hydrogenchloride / 1,4-dioxane / 4 h / 0 - 20 °C / Inert atmosphere
2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; methanol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
1,4-dioxane; N,N-dimethyl-formamide;