N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine

Base Information

• Chemical Name: N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine
• CAS No.: 934416-02-1
• Molecular Formula: C₂₁H₁₇N₅O₃S
• Molecular Weight: 419.464

Synonyms:N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine

Chemical Property of N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine

Chemical Property:

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Technology Process of N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine

There total 2 articles about N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

N-[1-(3-Azido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide (934416-00-9) → N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine (934416-02-1)

Guidance literature:

With lead(IV) acetate; In acetic acid; at 20 ℃;

DOI:10.1134/S1070428006060108

Reference yield:

N-(2,6-dimethyl-4-oxocyclohexa-2,5-dienylidene)-N'-(phenylsulfonyl)benzimidamide (308291-71-6) → N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine (934416-02-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / sodium azide / acetic acid / 1 h / 20 °C

2: 79 percent / lead tetraacetate / acetic acid / 20 °C

With lead(IV) acetate; sodium azide; In acetic acid;

DOI:10.1134/S1070428006060108

Reference yield: 64.0%

N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine (934416-02-1) → N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide (934416-04-3)

Guidance literature:

With sodium azide; In acetic acid; at 20 ℃; for 1h;

DOI:10.1134/S1070428006060108

upstream raw materials:

N-[1-(3-Azido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

N-(2,6-dimethyl-4-oxocyclohexa-2,5-dienylidene)-N'-(phenylsulfonyl)benzimidamide

Downstream raw materials:

N-(N-phenylsulfonylbenzimidoyl)-4-amino-2-azido-6-chloro-3,5-dimethylphenol

N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

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