N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

Base Information

Chemical Name:N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide
CAS No.:934416-04-3
Molecular Formula:C₂₁H₁₈N₈O₃S
Molecular Weight:462.492
Hs Code.:

Synonyms:N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

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Chemical Property of N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

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Technology Process of N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

There total 3 articles about N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 934416-02-1
N-(N-phenylsulfonylbenzimidoyl)-2-azido-3,5-dimethyl-1,4-benzoquinone imine

: 934416-04-3
N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

Guidance literature:: With sodium azide; In acetic acid; at 20 ℃; for 1h;
DOI:10.1134/S1070428006060108

Reference yield:

: 934416-00-9
N-[1-(3-Azido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

: 934416-04-3
N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / lead tetraacetate / acetic acid / 20 °C

2: 64 percent / sodium azide / acetic acid / 1 h / 20 °C

With lead(IV) acetate; sodium azide; In acetic acid;
DOI:10.1134/S1070428006060108

Reference yield:

: 308291-71-6
N-(2,6-dimethyl-4-oxocyclohexa-2,5-dienylidene)-N'-(phenylsulfonyl)benzimidamide

: 934416-04-3
N-[1-(3,5-Diazido-4-hydroxy-2,6-dimethyl-phenylamino)-1-phenyl-meth-(E)-ylidene]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / sodium azide / acetic acid / 1 h / 20 °C

2: 79 percent / lead tetraacetate / acetic acid / 20 °C

3: 64 percent / sodium azide / acetic acid / 1 h / 20 °C

With lead(IV) acetate; sodium azide; In acetic acid;
DOI:10.1134/S1070428006060108