[methyl 4-(10,15,20-triphenylporphyrin-5-yl-^κ4N^21,22,23,24)benzoato(2-)]copper

Base Information

• Chemical Name: [methyl 4-(10,15,20-triphenylporphyrin-5-yl-^κ4N^21,22,23,24)benzoato(2-)]copper
• CAS No.: 202007-74-7
• Molecular Formula: C₄₆H₃₀CuN₄O₂
• Molecular Weight: 734.316

Synonyms:[methyl 4-(10,15,20-triphenylporphyrin-5-yl-^κ4N^21,22,23,24)benzoato(2-)]copper

Chemical Property of [methyl 4-(10,15,20-triphenylporphyrin-5-yl-^κ4N^21,22,23,24)benzoato(2-)]copper

Chemical Property:

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Technology Process of [methyl 4-(10,15,20-triphenylporphyrin-5-yl-^κ4N^21,22,23,24)benzoato(2-)]copper

There total 2 articles about [methyl 4-(10,15,20-triphenylporphyrin-5-yl-^κ4N^21,22,23,24)benzoato(2-)]copper which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

copper(II) acetate monohydrate (6046-93-1) + 5-(4-methoxycarbonylphenyl)-10,15,20-triphenyl-21H,23H-porphyrin → [methyl 4-(10,15,20-triphenylporphyrin-5-yl-κ4N21,22,23,24)benzoato(2-)]copper (202007-74-7)

Guidance literature:

In methanol; dichloromethane; at 24 ℃; for 16h;

DOI:10.1021/jacs.1c02417

Reference yield: 94.0%

5,10,15-triphenyl-20-(4-methoxycarbonylphenyl)porphyrin → [methyl 4-(10,15,20-triphenylporphyrin-5-yl-κ4N21,22,23,24)benzoato(2-)]copper (202007-74-7)

Guidance literature:

With copper(II) acetate monohydrate; In methanol; chloroform; for 2h; Reflux;

DOI:10.1142/S1088424611003379

Reference yield: 88.0%

bis(cyclopentadienyl)-titanium(III) chloride + [methyl 4-(10,15,20-triphenylporphyrin-5-yl-κ4N21,22,23,24)benzoato(2-)]copper (202007-74-7) → μ-[4-(10,15,20-triphenylporphyrin-5-yl-2κ4N21,22,23,24)benzoato(3-)-1κ2O,O’]-bis(1η5-cyclopentadienyl)titaniumcopper

Guidance literature:

[methyl 4-(10,15,20-triphenylporphyrin-5-yl-^κ4N^21,22,23,24)benzoato(2-)]copper; With potassium hydroxide; In tetrahydrofuran; ethanol; water; at 66 ℃; for 16h;

With hydrogenchloride; In water; pH=3;

bis(cyclopentadienyl)-titanium(III) chloride; With 2,6-dimethylpyridine; In tetrahydrofuran; for 1h; Glovebox; Inert atmosphere;

DOI:10.1021/jacs.1c02417

upstream raw materials:

copper(II) acetate monohydrate

Downstream raw materials:

C₄₆H₂₂Br₈CuN₄O₂

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