4-decylphenylnitromethane

Base Information

Chemical Name:4-decylphenylnitromethane
CAS No.:162359-26-4
Molecular Formula:C₁₇H₂₇NO₂
Molecular Weight:277.407
Hs Code.:

Synonyms:4-decylphenylnitromethane

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Chemical Property of 4-decylphenylnitromethane

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Technology Process of 4-decylphenylnitromethane

There total 5 articles about 4-decylphenylnitromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 162359-25-3
4-decylbenzyl bromide

: 162359-26-4
4-decylphenylnitromethane

Guidance literature:: With silver(I) nitrite; In diethyl ether; at 0 ℃; for 4h;
DOI:10.1021/jm000173z

Reference yield:

: 104-72-3
decylbenzene

: 162359-26-4
4-decylphenylnitromethane

Guidance literature:: Multi-step reaction with 4 steps

1: TiCl₄ / CH₂Cl₂ / 1 h / 20 °C

2: 56 percent / NaBH₄ / methanol; propan-2-ol / 0.17 h / 20 °C

3: 98 percent / 48percent aq. HBr / toluene / 24 h / 90 °C

4: 47 percent / AgNO₂ / diethyl ether / 4 h / 0 °C

With sodium tetrahydroborate; silver(I) nitrite; titanium tetrachloride; In methanol; diethyl ether; dichloromethane; isopropyl alcohol; toluene; 1: Formylation / 2: Reduction / 3: Bromination / 4: Nitration;
DOI:10.1021/jm000173z

Reference yield:

: 70972-99-5
4-(n-decyl)benzaldehyde

: 162359-26-4
4-decylphenylnitromethane

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / NaBH₄ / methanol; propan-2-ol / 0.17 h / 20 °C

2: 98 percent / 48percent aq. HBr / toluene / 24 h / 90 °C

3: 47 percent / AgNO₂ / diethyl ether / 4 h / 0 °C

With sodium tetrahydroborate; silver(I) nitrite; In methanol; diethyl ether; isopropyl alcohol; toluene; 1: Reduction / 2: Bromination / 3: Nitration;
DOI:10.1021/jm000173z