S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate

Base Information

• Chemical Name: S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate
• CAS No.: 1068659-39-1
• Molecular Formula: C₃₂H₃₂ClO₅PS
• Molecular Weight: 595.096

Synonyms:S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate

Chemical Property of S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate

Chemical Property:

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Technology Process of S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate

There total 1 articles about S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-3-(trityloxy)propanoic acid (1036914-96-1) + O-phenyl phosphorodichloridate (770-12-7) → S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate (1068659-39-1)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1016/j.bmc.2008.06.024

Reference yield: 72.0%

S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl phenyl phosphorochloridate (1068659-39-1) + 3'-azido-2',3'-deoxythymidine (30516-87-1,399024-19-2) → O-(3'-azido-2',3'-dideoxythymidin-5'-yl)-O'-[S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl]-O''-phenyl phosphate (1068659-43-7)

Guidance literature:

With 1-methyl-1H-imidazole; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1016/j.bmc.2008.06.024

upstream raw materials:

2,2-dimethyl-3-(trityloxy)propanoic acid

O-phenyl phosphorodichloridate

Downstream raw materials:

O-(3'-azido-2',3'-dideoxythymidin-5'-yl)-O'-[S-(2,2-dimethyl-3-(triphenylmethoxy)propionyl)thioethyl]-O''-phenyl phosphate

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