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Phenyl dichlorophosphate
Cas No: 770-12-7
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
Phenyl dichlorophosphate
Cas No: 770-12-7
USD $ 100.0-600.0 / Gram 10 Gram 500 Metric Ton/Day GZ HONESTCHEM CO., LTD Contact Supplier
High quality Monophenyl Dichlorophosphate (Mpcp) supplier in China
Cas No: 770-12-7
No Data No Data Metric Ton/Day Simagchem Corporation Contact Supplier
Phenyl dichlorophosphate
Cas No: 770-12-7
USD $ 1.0-2.0 / Metric Ton 1 Metric Ton 100 Metric Ton/Week Hebei yanxi chemical co.,LTD. Contact Supplier
Phenyl dichlorophosphate 770-12-7
Cas No: 770-12-7
No Data 25 Kilogram 5000 Metric Ton/Month Hefei TNJ chemical industry co.,ltd Contact Supplier
Phenylphosphoryl dichloride
Cas No: 770-12-7
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
Phenyl phosphorodichloridate, 97%
Cas No: 770-12-7
No Data 1 Gram 20 Metric Ton/Week Henan Allgreen Chemical Co.,Ltd Contact Supplier
Factory Supply Phenyl phosphorodichloridate
Cas No: 770-12-7
No Data 1 1 Ality Chemical Corporation Contact Supplier
Amadis Chemical offer CAS#770-12-7;CAT#A838943
Cas No: 770-12-7
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
Phenyl dichlorophosphate CAS: 770-12-7
Cas No: 770-12-7
USD $ 1.0-2.0 / Metric Ton 5 Metric Ton 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier

770-12-7 Usage

Health Hazard

TOXIC; inhalation, ingestion or skin contact with material may cause severe injury or death. Contact with molten substance may cause severe burns to skin and eyes. Avoid any skin contact. Effects of contact or inhalation may be delayed. Fire may produce irritating, corrosive and/or toxic gases. Runoff from fire control or dilution water may be corrosive and/or toxic and cause pollution.

General Description

A liquid. May severely irritate skin, eyes and mucous membranes.

Reactivity Profile

An hologenated organophosphate. Organophosphates are susceptible to formation of highly toxic and flammable phosphine gas in the presence of strong reducing agents such as hydrides. Partial oxidation by oxidizing agents may result in the release of toxic phosphorus oxides.

Chemical Properties

clear colourless to very slightly brown liquid

Uses

In organic synthesis for preparation of lactams, phosphate diesters and for oxidation reactions.

Fire Hazard

Non-combustible, substance itself does not burn but may decompose upon heating to produce corrosive and/or toxic fumes. Some are oxidizers and may ignite combustibles (wood, paper, oil, clothing, etc.). Contact with metals may evolve flammable hydrogen gas. Containers may explode when heated.

Air & Water Reactions

About the same density as water and moderately soluble in water.
InChI:InChI=1/C6H5Cl2O2P/c7-11(8,9)10-6-4-2-1-3-5-6/h1-5H

770-12-7 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (P0209)  Phenyl Dichlorophosphate  >98.0%(GC)(T) 770-12-7 25g 250.00CNY Detail
TCI America (P0209)  Phenyl Dichlorophosphate  >98.0%(GC)(T) 770-12-7 500g 2,330.00CNY Detail
Alfa Aesar (A10479)  Phenyl phosphorodichloridate, 97%    770-12-7 25g 168.0CNY Detail
Alfa Aesar (A10479)  Phenyl phosphorodichloridate, 97%    770-12-7 100g 477.0CNY Detail
Alfa Aesar (A10479)  Phenyl phosphorodichloridate, 97%    770-12-7 500g 2204.0CNY Detail
Aldrich (P22389)  Phenyldichlorophosphate  ≥95% 770-12-7 P22389-25G 284.31CNY Detail
Aldrich (P22389)  Phenyldichlorophosphate  ≥95% 770-12-7 P22389-100G 748.80CNY Detail

770-12-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Phenyl dichlorophosphate

1.2 Other means of identification

Product number -
Other names Phenylphosphoric dichloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:770-12-7 SDS

770-12-7Synthetic route

phenyl phosphorodichloridite
3426-89-9

phenyl phosphorodichloridite

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With ozone In dichloromethane at 0℃;99%
phenol
108-95-2

phenol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With triethylamine; trichlorophosphate In tert-butyl methyl ether at -55 - 20℃; for 4h;98%
With magnesium chloride; trichlorophosphate at 80 - 95℃; for 5h; Large scale;91.5%
With triethylamine; trichlorophosphate In diethyl ether at -78 - 20℃; Inert atmosphere;85%
sodium phenoxide
139-02-6

sodium phenoxide

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With tetrabutylammomium bromide; trichlorophosphate In toluene for 1h;90%
tetrachlorophenoxyphosphorane
19579-04-5

tetrachlorophenoxyphosphorane

ethyl vinyl ether
109-92-2

ethyl vinyl ether

A

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

B

phenyl (2-ethoxyvinyl)-phosphonochloridate

phenyl (2-ethoxyvinyl)-phosphonochloridate

Conditions
ConditionsYield
With sulfur dioxide In benzene at 0 - 5℃;A 32.5%
B 67.1%
phenol
108-95-2

phenol

A

phosphoric acid triphenyl ester
115-86-6

phosphoric acid triphenyl ester

B

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C

chlorophosphoric acid diphenyl ester
2524-64-3

chlorophosphoric acid diphenyl ester

Conditions
ConditionsYield
With magnesium chloride; trichlorophosphate In xylene at 90 - 110℃; Kinetics; Product distribution; Rate constant;
With trichlorophosphate at 102 - 240℃;
phenyl sulfate potassium

phenyl sulfate potassium

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With phosphorus pentachloride
phosphoric acid phenyl ester tetrachloride

phosphoric acid phenyl ester tetrachloride

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With sulfur dioxide
phenol
108-95-2

phenol

phosphorous oxychloride

phosphorous oxychloride

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With triethylamine In diethyl ether at 0℃; for 0.5h; Yield given;
phenol
108-95-2

phenol

A

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

B

phosphoric acid diphenyl ester chloride , triphenyl phosphate

phosphoric acid diphenyl ester chloride , triphenyl phosphate

Conditions
ConditionsYield
With trichlorophosphate
phosphorus trichloride
7719-12-2, 52843-90-0

phosphorus trichloride

phenol
108-95-2

phenol

A

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

B

chlorophosphoric acid diphenyl ester
2524-64-3

chlorophosphoric acid diphenyl ester

Conditions
ConditionsYield
at 140℃;
diethyl amine hydrochloride
660-68-4

diethyl amine hydrochloride

phenol
108-95-2

phenol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With trichlorophosphate
phenol
108-95-2

phenol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
In not given react. of POCl3 with C6H5OH;;
In not given react. of POCl3 with C6H5OH;;
phenol
108-95-2

phenol

A

Phenylchlorophosphonic Acid Phenyl Ester
61274-57-5

Phenylchlorophosphonic Acid Phenyl Ester

B

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Conditions
ConditionsYield
With titanium tetrachloride; trichlorophosphate at 70 - 90℃; Reagent/catalyst; Temperature; Overall yield = 95 %;
O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phosphoric acid monophenyl ester
701-64-4

phosphoric acid monophenyl ester

Conditions
ConditionsYield
With silver nitrate In acetonitrile at 0 - 5℃; for 1h; Hydrolysis;100%
With water at 20℃;
With diethyl ether; water
L-alanine benzyl ester hydrochloride
5557-81-3, 5557-83-5, 34404-37-0

L-alanine benzyl ester hydrochloride

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl(benzyloxy-L-alaninyl)phosphorochloridate
183370-70-9

phenyl(benzyloxy-L-alaninyl)phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78℃; for 1h; Inert atmosphere;100%
With triethylamine In dichloromethane at -80 - 20℃;98%
With triethylamine In dichloromethane at -78 - 20℃; for 2.5h; Inert atmosphere;95%
O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

alanine isopropyl ester hydrochloride
39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

phenyl(isopropoxy-L-alaninyl) phosphorochloridate
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

Conditions
ConditionsYield
With triethylamine In tert-butyl methyl ether at -65 - -50℃; for 2h; Inert atmosphere; Cooling with acetone-dry ice;100%
With triethylamine In tert-butyl methyl ether at -55℃; for 2h;100%
With triethylamine In dichloromethane at -78 - 20℃; for 2.5h; Inert atmosphere;93%
3-((4-cyclobutylbutyl)sulfonyl)propan-1-ol

3-((4-cyclobutylbutyl)sulfonyl)propan-1-ol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

3-((4-cyclobutylbutyl)sulfonyl)propyl phenyl (S)-phosphorochloridate

3-((4-cyclobutylbutyl)sulfonyl)propyl phenyl (S)-phosphorochloridate

Conditions
ConditionsYield
With 2,6-dimethylpyridine In tetrahydrofuran at 0 - 20℃; for 18h;100%
phthalyl alcohol
612-14-6

phthalyl alcohol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

2-phenoxy-2-oxo-5,6-benzo-1,3,2-dioxaphosphepane
49785-03-7

2-phenoxy-2-oxo-5,6-benzo-1,3,2-dioxaphosphepane

Conditions
ConditionsYield
With triethylamine In ethyl acetate for 48h;99.5%
O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

(S)-1-isopropylallylamine hydrochloride

(S)-1-isopropylallylamine hydrochloride

(NHC6H11)2PO2C6H5
345898-62-6

(NHC6H11)2PO2C6H5

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane for 3.5h;99%
With dmap; triethylamine In dichloromethane Heating;
(L)-phenylalanine ethyl ester hydrochloride
3182-93-2

(L)-phenylalanine ethyl ester hydrochloride

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

(2S)-ethyl 2-(((RS)-chloro(phenoxy)phosphoryl)amino)-3-phenylpropanoate
287478-21-1

(2S)-ethyl 2-(((RS)-chloro(phenoxy)phosphoryl)amino)-3-phenylpropanoate

Conditions
ConditionsYield
Stage #1: (L)-phenylalanine ethyl ester hydrochloride; O-phenyl phosphorodichloridate In dichloromethane at -78℃; Inert atmosphere;
Stage #2: With triethylamine In dichloromethane at -78 - 20℃;
99%
With triethylamine In dichloromethane at -78 - 20℃;72%
With triethylamine In dichloromethane at -78 - 20℃; for 1.25h;
L-isoleucine benzyl ester tosylate
16652-75-8

L-isoleucine benzyl ester tosylate

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl-(benzoxy-L-isoleucinyl)-phosphorochloridate
1184942-63-9

phenyl-(benzoxy-L-isoleucinyl)-phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; Inert atmosphere;99%
isopropyl L-alanine
39825-33-7

isopropyl L-alanine

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl(isopropoxy-L-alaninyl) phosphorochloridate
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; for 1.25h; Inert atmosphere;99%
With triethylamine In dichloromethane78%
With N-ethyl-N,N-diisopropylamine In dichloromethane at -80℃; for 2h;
(S)-[1,1']-binaphthalenyl-2,2'-diol
18531-99-2

(S)-[1,1']-binaphthalenyl-2,2'-diol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C26H17O4P

C26H17O4P

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; Sealed tube;99%
With triethylamine In dichloromethane at 23℃; for 18h;63%
H-Phe-OEt
3081-24-1

H-Phe-OEt

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

(2S)-ethyl 2-(((RS)-chloro(phenoxy)phosphoryl)amino)-3-phenylpropanoate
287478-21-1

(2S)-ethyl 2-(((RS)-chloro(phenoxy)phosphoryl)amino)-3-phenylpropanoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; for 1.25h; Inert atmosphere;99%
L-Leucine benzyl ester
1738-69-8

L-Leucine benzyl ester

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl-(benzoxy-L-leucinyl)-phosphorochloridate
840506-65-2

phenyl-(benzoxy-L-leucinyl)-phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; for 1.25h; Inert atmosphere;99%
L-alanine methyl ester hydrochloride
2491-20-5

L-alanine methyl ester hydrochloride

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl methoxyalaninyl phosphorochloridate
142629-80-9

phenyl methoxyalaninyl phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -80 - 20℃;98%
With triethylamine In dichloromethane at -78 - 20℃; for 1h;92%
With triethylamine In dichloromethane at -78 - 20℃; for 2.5h; Inert atmosphere;91%
L-Leucine ethyl ester
2743-60-4

L-Leucine ethyl ester

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl (ethyloxy-L-leucinyl)phosphorochloridate
926308-86-3

phenyl (ethyloxy-L-leucinyl)phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; for 1.25h; Inert atmosphere;98%
L-isoleucine ethyl ester
921-74-4

L-isoleucine ethyl ester

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

ethyl (chloro(phenoxy)phosphoryl)-L-isoleucinate
926309-00-4

ethyl (chloro(phenoxy)phosphoryl)-L-isoleucinate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; for 1.25h; Inert atmosphere;98%
6-chloro-2-hydroxypyridine
16879-02-0

6-chloro-2-hydroxypyridine

isopropyl L-alanine
39825-33-7

isopropyl L-alanine

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C17H20ClN2O5P

C17H20ClN2O5P

Conditions
ConditionsYield
Stage #1: isopropyl L-alanine; O-phenyl phosphorodichloridate With N-ethyl-N,N-diisopropylamine In dichloromethane at -50 - -5℃; Inert atmosphere;
Stage #2: 6-chloro-2-hydroxypyridine With N-ethyl-N,N-diisopropylamine In dichloromethane at -10 - 0℃; Inert atmosphere;
97.5%
5-bromopyridine-3-ol
74115-13-2

5-bromopyridine-3-ol

isopropyl L-alanine
39825-33-7

isopropyl L-alanine

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C17H20BrN2O5P

C17H20BrN2O5P

Conditions
ConditionsYield
Stage #1: isopropyl L-alanine; O-phenyl phosphorodichloridate With triethylamine In dichloromethane at -50 - -5℃; Inert atmosphere;
Stage #2: 5-bromopyridine-3-ol With triethylamine In dichloromethane at -10 - 0℃; Inert atmosphere;
97.3%
2,2,3,3,4,4,5,5,5-nonafluoropentanol
355-28-2

2,2,3,3,4,4,5,5,5-nonafluoropentanol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Phosphoric acid bis-(2,2,3,3,4,4,5,5,5-nonafluoro-pentyl) ester phenyl ester
70508-50-8

Phosphoric acid bis-(2,2,3,3,4,4,5,5,5-nonafluoro-pentyl) ester phenyl ester

Conditions
ConditionsYield
With lithium chloride for 4h; bath temperature 180 deg C;97%
With calcium chloride at 120℃;
2-chloropyridin-4-ol
17368-12-6

2-chloropyridin-4-ol

isopropyl L-alanine
39825-33-7

isopropyl L-alanine

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C17H20ClN2O5P

C17H20ClN2O5P

Conditions
ConditionsYield
Stage #1: isopropyl L-alanine; O-phenyl phosphorodichloridate With N-ethyl-N,N-diisopropylamine In dichloromethane at -50 - -5℃; Inert atmosphere;
Stage #2: 2-chloropyridin-4-ol With N-ethyl-N,N-diisopropylamine In dichloromethane at -10 - 0℃; Inert atmosphere;
97%
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride
7524-50-7

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl methoxyphenylalaninyl phosphorochloridate
147907-42-4

phenyl methoxyphenylalaninyl phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -70 - 20℃;96.7%
With triethylamine In dichloromethane at -78 - 20℃;
With triethylamine In dichloromethane at -78 - 20℃;
With triethylamine In dichloromethane at -78 - 20℃;
O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

(S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol
39648-74-3, 65355-00-2, 65355-14-8

(S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol

C26H25O4P

C26H25O4P

Conditions
ConditionsYield
Stage #1: (S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Sealed tube;
Stage #2: O-phenyl phosphorodichloridate In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Sealed tube;
96%
methyl O-(1,1-dimethylethyl)-L-threoninate hydrochloride
71989-43-0

methyl O-(1,1-dimethylethyl)-L-threoninate hydrochloride

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

phenyl-(methoxy-O-tert-butyl-L-threoninyl) phosphorochloridate

phenyl-(methoxy-O-tert-butyl-L-threoninyl) phosphorochloridate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; for 1.5h;96%
benzyl 2-aminoisobutyrate
55456-40-1

benzyl 2-aminoisobutyrate

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

benzyl 2-((chloro(phenoxy)phosphoryl)amino)-2-methylpropanoate
840506-42-5

benzyl 2-((chloro(phenoxy)phosphoryl)amino)-2-methylpropanoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78 - 20℃; for 1.25h; Inert atmosphere;96%
5-chloropyridin-3-ol
74115-12-1

5-chloropyridin-3-ol

isopropyl L-alanine
39825-33-7

isopropyl L-alanine

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C17H20ClN2O5P

C17H20ClN2O5P

Conditions
ConditionsYield
Stage #1: isopropyl L-alanine; O-phenyl phosphorodichloridate With triethylamine In dichloromethane at -50 - -5℃; Inert atmosphere;
Stage #2: 5-chloropyridin-3-ol With triethylamine In dichloromethane at -10 - 0℃; Inert atmosphere;
95.7%
N-(4-hydroxyphenyl)maleimide
7300-91-6

N-(4-hydroxyphenyl)maleimide

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C26H17N2O8P

C26H17N2O8P

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 5 - 7℃; Temperature;95.3%
2,2,2-trifluoroethanol
75-89-8

2,2,2-trifluoroethanol

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

Phosphoric acid phenyl ester bis-(2,2,2-trifluoro-ethyl) ester

Phosphoric acid phenyl ester bis-(2,2,2-trifluoro-ethyl) ester

Conditions
ConditionsYield
With lithium chloride for 8h; bath temperature 160 - 170 deg C;95.2%
for 24h; Alkaline conditions;
O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

cyclohexanol
108-93-0

cyclohexanol

dicyclohexyl phenyl phosphate

dicyclohexyl phenyl phosphate

Conditions
ConditionsYield
With molybdenum(VI) tetrachloride oxide; triethylamine In dichloromethane at 20℃;95%
at 70 - 80℃;
Allylbenzylamine
4383-22-6

Allylbenzylamine

O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

C16H17ClNO2P
920526-13-2

C16H17ClNO2P

Conditions
ConditionsYield
Stage #1: O-phenyl phosphorodichloridate With dmap; triethylamine In dichloromethane at 20℃; for 0.25h;
Stage #2: Allylbenzylamine In dichloromethane at 20℃; for 3h;
95%
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