diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate

Base Information

Chemical Name:diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate
CAS No.:1366126-17-1
Molecular Formula:C₂₈H₂₁F₇NO₃P
Molecular Weight:583.442
Hs Code.:

Synonyms:diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate

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Technology Process of diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate

There total 2 articles about diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 313-72-4
octafluoronaphthalene

: 122570-91-6
diethyl N-(diphenylmethylene) aminomethyl phosphonate

: 1366126-17-1
diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate

Guidance literature:: octafluoronaphthalene; diethyl N-(diphenylmethylene) aminomethyl phosphonate; With potassium hydride; In tetrahydrofuran; paraffin oil; at 0 ℃; Inert atmosphere;

With acetic acid; In tetrahydrofuran; paraffin oil; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.jfluchem.2012.01.004

Reference yield:

: 50917-72-1
aminomethylphosphonic acid diethyl ester

: 1366126-17-1
diethyl (diphenylmethyleneamino)(1,3,4,5,6,7,8-heptafluoro-2-naphthyl)methanephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzene / 48 h / 10 - 20 °C / Inert atmosphere

2.1: potassium hydride / tetrahydrofuran; paraffin oil / 0 °C / Inert atmosphere

2.2: Inert atmosphere

With potassium hydride; In tetrahydrofuran; paraffin oil; benzene;
DOI:10.1016/j.jfluchem.2012.01.004