N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

Base Information

Chemical Name:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide
CAS No.:1449203-94-4
Molecular Formula:C₁₇H₂₂IN₃O₃S
Molecular Weight:475.35
Hs Code.:

Synonyms:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

Suppliers and Price of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

There total 6 articles about N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.46%

: C₂₅H₃₆IN₃O₄S

: 1449203-94-4
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

Guidance literature:: With methanol; sodium hydroxide; for 3h; Reflux;

Reference yield:

: 5438-36-8
5-iodovaniline

: 1449203-94-4
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 4 h / 20 °C

2.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

3.1: iron(III) chloride / methanol; water / Reflux

3.2: 1 h / Reflux

4.1: pyridine / 2 h / 20 °C

5.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; sulfuric acid; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001

Reference yield:

: 486994-14-3
4-(acetyloxy)-3-iodo-5-methoxybenzaldehyde

: 1449203-94-4
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl]-octanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

2.1: iron(III) chloride / methanol; water / Reflux

2.2: 1 h / Reflux

3.1: pyridine / 2 h / 20 °C

4.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001