N-(cyclohex-2-en-1-yl)-N-methylamine

Base Information

• Chemical Name: N-(cyclohex-2-en-1-yl)-N-methylamine
• CAS No.: 86766-74-7
• Molecular Formula: C₇H₁₃N
• Molecular Weight: 111.187
• Mol file: 86766-74-7.mol

Synonyms:N-(cyclohex-2-en-1-yl)-N-methylamine

Chemical Property of N-(cyclohex-2-en-1-yl)-N-methylamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-(cyclohex-2-en-1-yl)-N-methylamine

There total 11 articles about N-(cyclohex-2-en-1-yl)-N-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

rac-3-bromocyclohexene (1521-51-3,113667-32-6) + methylamine (74-89-5) → N-(cyclohex-2-en-1-yl)-N-methylamine (86766-74-7)

Guidance literature:

In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/op500173q

Reference yield: 85.0%

N-Cyclohex-2-enyl-N-methyl-hydroxylamine (118149-88-5) → N-(cyclohex-2-en-1-yl)-N-methylamine (86766-74-7)

Guidance literature:

With hydrogenchloride; zinc; In water; at 80 ℃; for 1h;

DOI:10.1016/0040-4039(88)85061-5

Reference yield: 80.0%

N-(cyclohex-2-enyl) methyl carbamate (86766-64-5) → N-(cyclohex-2-en-1-yl)-N-methylamine (86766-74-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 4h; Heating;

DOI:10.1021/jo00168a040

upstream raw materials:

3-<(ethoxycarbonyl)amino>cyclohexene

rac-3-bromocyclohexene

methylamine

2,2,2-trichloro-N-cyclohex-2-en-1-yl-N-methylacetamide