4-bromobenzyl benzoate

Base Information

• Chemical Name: 4-bromobenzyl benzoate
• CAS No.: 38612-13-4
• Molecular Formula: C₁₄H₁₁BrO₂
• Molecular Weight: 291.144
• Mol file: 38612-13-4.mol

Synonyms:4-bromobenzyl benzoate

Chemical Property of 4-bromobenzyl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-bromobenzyl benzoate

There total 12 articles about 4-bromobenzyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(4-bromobenzyl)dimethylamine (6274-57-3) + dimethyl acetylenedicarboxylate (762-42-5) + benzoic acid (65-85-0,8013-63-6) → 1-dimethylamino-1,2-di(methoxycarbonyl)ethene (67751-25-1) + 4-bromobenzyl benzoate (38612-13-4)

Guidance literature:

In dichloromethane; at 20 ℃; for 24h; Time;

DOI:10.1016/j.tet.2012.08.024

Reference yield: 93.0%

4-bromobenzenemethanol (873-75-6) + benzoyl chloride (98-88-4) → 4-bromobenzyl benzoate (38612-13-4)

Guidance literature:

With pyridine; at 0 ℃; for 1.5h;

DOI:10.1016/j.bmc.2008.03.056

Reference yield: 77.0%

4-bromobenzenemethanol (873-75-6) + 1,3-diphenylpropanedione (120-46-7,61346-73-4) → 4-bromobenzyl 2-oxo-2-phenylacetate + 4-bromobenzyl benzoate (38612-13-4)

Guidance literature:

With pyridine; oxygen; copper(I) bromide; In toluene; at 90 ℃; for 18h; under 760.051 Torr; Schlenk technique;

DOI:10.1021/ja4085463

upstream raw materials:

sodium benzoate

1-bromomethyl-4-bromobenzene

4-bromobenzenemethanol

benzoyl chloride

Downstream raw materials:

4-cyanobenzyl benzoate

lorsartan

2-butyl-3-{4-[2-(1H-tetrazol-5-yl)phenyl]benzyl}-1,3-diazaspiro[4.4]non-1-en-4-one

N-pentanoyl-N-[[2'-(1H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl]-methyl]-(L)-valine