(2S,3S)-3-Hydroxy-2-methyl-3-phenyl-thiopropionic acid S-tert-butyl ester

Base Information

• Chemical Name: (2S,3S)-3-Hydroxy-2-methyl-3-phenyl-thiopropionic acid S-tert-butyl ester
• CAS No.: 112346-46-0
• Molecular Formula: C₁₄H₂₀O₂S
• Molecular Weight: 252.378

Synonyms:(2S,3S)-3-Hydroxy-2-methyl-3-phenyl-thiopropionic acid S-tert-butyl ester

Chemical Property of (2S,3S)-3-Hydroxy-2-methyl-3-phenyl-thiopropionic acid S-tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (2S,3S)-3-Hydroxy-2-methyl-3-phenyl-thiopropionic acid S-tert-butyl ester

There total 32 articles about (2S,3S)-3-Hydroxy-2-methyl-3-phenyl-thiopropionic acid S-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

prop-1-en-1-one (6004-44-0) + benzaldehyde (100-52-7) + 2-methylpropan-2-thiol (75-66-1) → threo-S-(1,1-dimethylethyl) 3-hydroxy-2-methyl-3-phenylpropanethioate (71908-06-0,71908-07-1,108033-37-0,108033-38-1,112346-46-0,112346-47-1,137942-04-2,137942-05-3) + erythro-S-(1,1-dimethylethyl) 3-hydroxy-2-methyl-3-phenylpropanethioate (71908-06-0,71908-07-1,108033-37-0,108033-38-1,112346-46-0,112346-47-1,137942-04-2,137942-05-3)

Guidance literature:

With bis(methylcyclopentadienyl) tin; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) THF, room temp., 20 min; 2) THF, -78 deg C, 2 h;

DOI:10.1246/cl.1986.213

Reference yield:

prop-1-en-1-one (6004-44-0) + benzaldehyde (100-52-7) + 2-methylpropan-2-thiol (75-66-1) → threo-S-(1,1-dimethylethyl) 3-hydroxy-2-methyl-3-phenylpropanethioate (71908-06-0,71908-07-1,108033-37-0,108033-38-1,112346-46-0,112346-47-1,137942-04-2,137942-05-3) + erythro-S-(1,1-dimethylethyl) 3-hydroxy-2-methyl-3-phenylpropanethioate (71908-06-0,71908-07-1,108033-37-0,108033-38-1,112346-46-0,112346-47-1,137942-04-2,137942-05-3)

Guidance literature:

With bis(methylcyclopentadienyl) tin; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) THF, room temp., 20 min; 2) THF, -78 deg C, 2 h;

DOI:10.1246/cl.1986.213

Reference yield:

prop-1-en-1-one (6004-44-0) + C12H27BS (43143-00-6) + benzaldehyde (100-52-7) → erythro-S-(1,1-dimethylethyl) 3-hydroxy-2-methyl-3-phenylpropanethioate (71908-06-0,71908-07-1,108033-37-0,108033-38-1,112346-46-0,112346-47-1,137942-04-2,137942-05-3)

Guidance literature:

Multistep reaction; (i) THF, (ii) /BRN= 1732373/, (iii) aq. H₂O₂;

DOI:10.1016/S0040-4039(01)93682-2

upstream raw materials:

tert-butyl thiopropionate

benzaldehyde

tert-Butyl-((E)-1-tert-butylsulfanyl-propenyloxy)-dimethyl-silane

1-tert-butylthio-1-(tert-butyldimethylsilyloxy)prop-1-ene

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