chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)

Base Information

Chemical Name:chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)
CAS No.:82456-65-3
Molecular Formula:C₅₄H₅₄CrN₆
Molecular Weight:839.059
Hs Code.:

chromium<sup>(0)</sup> hexakis(2,6-dimethylphenyl isocyanide)

Synonyms:chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)

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Chemical Property of chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)

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Technology Process of chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)

There total 2 articles about chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 10170-68-0,16997-54-9
trichlorotris(tetrahydrofuran)chromium(III)

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 82456-65-3
chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)

Guidance literature:: With Na#Hg; In tetrahydrofuran; soln. of Cr complex and isococyanide deriv. was added to Na amalgam (1,2%) and stirred for 3 h at room temp.; soln. was filtered, residue washed with THF, combined solns. were concd. and formed crystals dried under vac.; elem. anal.;
DOI:10.1016/0022-328X(85)87169-2

Reference yield:

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 82456-65-3
chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)

Guidance literature:: cobalt(II) chloride dihydrate;
DOI:10.1039/c39800000489

Reference yield: 91.0%

: 14104-20-2
silver tetrafluoroborate

: 82456-65-3
chromium⁽⁰⁾ hexakis(2,6-dimethylphenyl isocyanide)

: 85135-18-8
Cr(2,6-dimethylphenyl isocyanide)6BF₄

Guidance literature:: In acetone; Cr-complex in acetone was oxidized with AgBF4 according to Barybin, M. V. Ph.D.Dissertation, University of Minnesota, 1999;
DOI:10.1021/ja000212w