N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide

Base Information

Chemical Name:N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide
CAS No.:153906-09-3
Molecular Formula:C₁₂H₁₃Cl₂N₃O₃
Molecular Weight:318.16
Hs Code.:

Synonyms:N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide

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Chemical Property of N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide

Chemical Property:

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Technology Process of N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide

There total 3 articles about N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 598-41-4
H-Gly-NH₂

: 153906-08-2
N-(3,4-dichlorophenylacetyl)glycine

: 153906-09-3
N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Ambient temperature;
DOI:10.1021/jm00028a016

Reference yield:

: 5807-30-7
3,4-dichlorophenyl acetic acid

: 153906-09-3
N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 1-((dimethylamino)propyl)-3-ethylcarbodiimide hydrochloride, Et₃N / CH₂Cl₂ / Ambient temperature

2: 95 percent / 10percent KOH/MeOH / Ambient temperature

3: 72 percent / 1-((dimethylamino)propyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

With methanol; potassium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1021/jm00028a016

Reference yield:

: 153906-07-1
[2-(3,4-Dichloro-phenyl)-acetylamino]-acetic acid methyl ester

: 153906-09-3
N-[(Carbamoylmethyl-carbamoyl)-methyl]-2-(3,4-dichloro-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 10percent KOH/MeOH / Ambient temperature

2: 72 percent / 1-((dimethylamino)propyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

With methanol; potassium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/jm00028a016