5-cyclohexylisophthalic acid dimethyl ester

Base Information

Chemical Name:5-cyclohexylisophthalic acid dimethyl ester
CAS No.:191232-31-2
Molecular Formula:C₁₆H₂₀O₄
Molecular Weight:276.332
Hs Code.:

Synonyms:5-cyclohexylisophthalic acid dimethyl ester

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Chemical Property of 5-cyclohexylisophthalic acid dimethyl ester

Chemical Property:

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Technology Process of 5-cyclohexylisophthalic acid dimethyl ester

There total 2 articles about 5-cyclohexylisophthalic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 4441-56-9
cyclohexylboronic acid

: 51760-21-5
dimethyl 5-bromoisophthalate

: 191232-31-2
5-cyclohexylisophthalic acid dimethyl ester

Guidance literature:: With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In toluene; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ml4004952

Reference yield:

: 110-82-7,25012-93-5
cyclohexane

: 1459-93-4
dimethyl Isophthalate

: 191232-31-2
5-cyclohexylisophthalic acid dimethyl ester

: 1332460-93-1
C₁₆H₂₀O₄

: C₁₆H₂₀O₄

Guidance literature:: With dodecacarbonyl-triangulo-triruthenium; di-tert-butyl peroxide; 1,4-di(diphenylphosphino)-butane; at 135 ℃; for 12h; under 760.051 Torr; regioselective reaction; Under air; Darkness;
DOI:10.1021/ol202081c