N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin

Base Information

• Chemical Name: N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin
• CAS No.: 103670-28-6
• Molecular Formula: C₃₁H₃₄N₂O₄S₂
• Molecular Weight: 562.754
• Mol file: 103670-28-6.mol

Synonyms:N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin

Chemical Property of N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin

There total 1 articles about N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

4,4’-methylenebis(N-p-tosylanilide) (74043-79-1) + ethyl iodide (75-03-6) → N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin (103670-28-6)

Guidance literature:

With sodium; In methanol; for 12h; Heating;

Reference yield: 75.0%

N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin (103670-28-6) → N,N’-(4,4’-methylenebis(4,1-phenylene))diacetamide (843-29-8)

Guidance literature:

With sodium; In butan-1-ol; for 3.5h; Heating;

Reference yield:

N,N'-Diethyl-N,N'-bis(p-tolylsulfonyl)-4,4'-methylendianilin (103670-28-6) → N,N'-Bis(cyanmethyl)-N,N'-diethyl-4,4'-methylendianilin (103670-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / Na / butan-1-ol / 3.5 h / Heating

2: 54 percent / N,N-diisopropylethylamine / CHCl₃ / 6 h / Heating

With sodium; N-ethyl-N,N-diisopropylamine; In chloroform; butan-1-ol;

upstream raw materials:

4,4’-methylenebis(N-p-tosylanilide)

ethyl iodide

Downstream raw materials:

N,N’-(4,4’-methylenebis(4,1-phenylene))diacetamide

N,N'-Bis(cyanmethyl)-N,N'-diethyl-4,4'-methylendianilin