Technology Process of C27H27F2N3O6
There total 8 articles about C27H27F2N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H29F2N3O6;
With
water; sodium hydroxide;
In
ethanol;
at 20 ℃;
for 2h;
With
hydrogenchloride;
In
ethanol; water;
pH=7;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid / toluene / 7 h / 90 °C
2.1: formic acid; sulfuric acid / toluene; water / 3 h / 20 °C
2.2: 5 °C
3.1: acetic acid / toluene / 1.5 h / 50 °C
4.1: sodium hydroxide; water / ethanol / 2 h / 20 °C
4.2: pH 7
With
formic acid; sulfuric acid; water; acetic acid; sodium hydroxide;
In
ethanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium tert-pentoxide / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere
1.2: 2 h / 0 - 20 °C
2.1: 1,4-dioxane / 6 h / 20 °C
3.1: sodium t-butanolate / 7 h / 25 - 30 °C / Inert atmosphere
3.2: 15 h / 20 °C
4.1: methanol / 6 h / Reflux
5.1: acetic acid / toluene / 7 h / 90 °C
6.1: formic acid; sulfuric acid / toluene; water / 3 h / 20 °C
6.2: 5 °C
7.1: acetic acid / toluene / 1.5 h / 50 °C
8.1: sodium hydroxide; water / ethanol / 2 h / 20 °C
8.2: pH 7
With
formic acid; sulfuric acid; water; sodium tert-pentoxide; acetic acid; sodium hydroxide; sodium t-butanolate;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; toluene;