Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine

Base Information

Chemical Name:Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine
CAS No.:214832-93-6
Molecular Formula:C₂₇H₄₃NO₃Si
Molecular Weight:457.729
Hs Code.:

Synonyms:Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine

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Chemical Property of Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine

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Technology Process of Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine

There total 3 articles about Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 152299-13-3
(2S)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-(dibenzylamino)butan-1-ol

: 6482-24-2
2-Bromoethyl methyl ether

: 214832-93-6
Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine

Guidance literature:: With dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; 1.) r.t., 4 h, 2.) 65 deg C, 20 h;
DOI:10.1055/s-1998-6100

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 214832-93-6
Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / Et₃N, DMAP / CH₂Cl₂ / 8 h / 40 °C

2: 44 percent / NaH, Bu₄NI, DMAP / tetrahydrofuran / 1.) r.t., 4 h, 2.) 65 deg C, 20 h

With dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1998-6100

Reference yield:

: 137428-32-1
(2S)-2-[bis(phenylmethyl)amino]-1,4-butanediol

: 214832-93-6
Dibenzyl-[(S)-3-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethyl)-propyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / Et₃N, DMAP / CH₂Cl₂ / 8 h / 40 °C

2: 44 percent / NaH, Bu₄NI, DMAP / tetrahydrofuran / 1.) r.t., 4 h, 2.) 65 deg C, 20 h

With dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1998-6100