N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide

Base Information

Chemical Name:N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide
CAS No.:1268265-95-7
Molecular Formula:C₁₆H₂₄N₂O₃SSi
Molecular Weight:352.53
Hs Code.:

Synonyms:N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide

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Chemical Property of N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide

Chemical Property:

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Technology Process of N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide

There total 2 articles about N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98623-16-6
2-(4-amino-phenyl)ethanesulfonic acid methylamide

: 1268265-95-7
N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; iodine / dichloromethane / 25 - 30 °C

2.1: dichloromethane / 1.5 h / 25 °C

3.1: copper(l) iodide; lithium chloride / N,N-dimethyl-formamide / 0.5 h / 25 °C

3.2: 25 °C

With copper(l) iodide; iodine; sodium hydrogencarbonate; lithium chloride; In dichloromethane; N,N-dimethyl-formamide; 3.2: Sonogashira Coupling;

Reference yield:

: 1200070-42-3
2-(4-amino-3-iodo-phenyl)ethanesulfonic acid methylamide

: 1268265-95-7
N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 1.5 h / 25 °C

2.1: copper(l) iodide; lithium chloride / N,N-dimethyl-formamide / 0.5 h / 25 °C

2.2: 25 °C

With copper(l) iodide; lithium chloride; In dichloromethane; N,N-dimethyl-formamide; 2.2: Sonogashira Coupling;

Reference yield:

: 1268265-95-7
N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide

: 98623-50-8
N-Methyl-1H-indole-5-ethanesulphonamide

Guidance literature:: N-[4-(2-{methylsulfamoyl}ethyl)-2-{2-(trimethylsilanyl)ethynyl}phenyl]acetamide; With potassium tert-butylate; In 1-methyl-pyrrolidin-2-one; at 25 - 85 ℃; Inert atmosphere;

With water; In 1-methyl-pyrrolidin-2-one; at 25 ℃; for 0.5h;