3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid

Base Information

Chemical Name:3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid
CAS No.:1197049-22-1
Molecular Formula:C₂₉H₂₆N₄O₂
Molecular Weight:462.551
Hs Code.:

Synonyms:3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid

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Chemical Property of 3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid

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Technology Process of 3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid

There total 2 articles about 3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1197049-17-4
C₂₈H₂₇BrN₄

: 1197049-22-1
3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid

Guidance literature:: C₂₈H₂₇BrN₄; With potassium tert-butylate; In tetrahydrofuran; at -25 - 20 ℃; Inert atmosphere;

carbon dioxide; In tetrahydrofuran; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 1197049-19-6
ethyl 3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolate

: 1197049-22-1
3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid

Guidance literature:: ethyl 3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolate; With ethanol; water; sodium hydroxide;

With hydrogenchloride; In water; pH=3; Product distribution / selectivity;

Reference yield: 68.0%

: 1197049-22-1
3-(4-((1,7'-dimethyl-2'-propyl-1H,3'H-2,5'-bibenzo[d]imidazol-3'-yl)methyl)phenyl)propiolic acid

: 74-86-2,25067-58-7
acetylene

: 144701-48-4
telmisatran

Guidance literature:: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; at 30 ℃; for 8h; Inert atmosphere;