C₂₇H₃₂N₂O₂

Base Information

• Chemical Name: C₂₇H₃₂N₂O₂
• CAS No.: 1417530-15-4
• Molecular Formula: C₂₇H₃₂N₂O₂
• Molecular Weight: 416.563
• Mol file: 1417530-15-4.mol

Synonyms:C₂₇H₃₂N₂O₂

Chemical Property of C₂₇H₃₂N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₇H₃₂N₂O₂

There total 1 articles about C₂₇H₃₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-methyltrityl chloride (23429-44-9) + Ser(tBu)-NH2 → C27H32N2O2 (1417530-15-4)

Guidance literature:

With pyridine; In dichloromethane; for 4h;

DOI:10.1002/chem.201201337

Reference yield: 73.0%

C27H32N2O2 (1417530-15-4) → C27H34N2O (1417529-77-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 48h;

DOI:10.1002/chem.201201337

Reference yield:

C27H32N2O2 (1417530-15-4) → C41H49N7O7 (1417530-41-6)

Guidance literature:

Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / diethyl ether / 48 h

2: triethylamine / dichloromethane / 3 h

3: N-ethyl-N,N-diisopropylamine; 2,6-dimethylpyridine; HATU / N,N-dimethyl-formamide / 12 h

4: lithium hydroxide / 1,4-dioxane; water / 2 h

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; In 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1002/chem.201201337

upstream raw materials:

4-methyltrityl chloride

Downstream raw materials:

C₂₇H₃₄N₂O

C₄₁H₄₉N₇O₇

C₃₆H₄₂N₄O₆