4-METHYLTRITYL CHLORIDE

Base Information

• Chemical Name: 4-METHYLTRITYL CHLORIDE
• CAS No.: 23429-44-9
• Molecular Formula: C20H17Cl
• Molecular Weight: 292.808
• Hs Code.: 2903999090
• European Community (EC) Number: 685-318-3
• DSSTox Substance ID: DTXSID10401468
• Nikkaji Number: J1.075.623E
• Wikidata: Q72492283
• Mol file: 23429-44-9.mol

Synonyms:4-Methyltrityl chlorid;

Chemical Property of 4-METHYLTRITYL CHLORIDE

Chemical Property:

• Vapor Pressure: 2.12E-06mmHg at 25°C
• Melting Point: 98-99 °C
• Refractive Index: 1.6
• Boiling Point: 405 °C at 760 mmHg
• Flash Point: 186.5 °C
• PSA: 0.00000
• Density: 1.124 g/cm³
• LogP: 5.52570
• Storage Temp.: -20°C
• XLogP3: 5.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 292.1018782
• Heavy Atom Count: 21
• Complexity: 286

Purity/Quality:

97% ^*data from raw suppliers

(Chloro(p-tolyl)methylene)dibenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)C(C2=CC=CC=C2)(C3=CC=CC=C3)Cl

Technology Process of 4-METHYLTRITYL CHLORIDE

There total 8 articles about 4-METHYLTRITYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(4-methylphenyl)diphenylmethanol (5440-76-6) → 4-methyltrityl chloride (23429-44-9)

Guidance literature:

With acetyl chloride; at 50 ℃; for 1h;

Reference yield:

para-bromotoluene (106-38-7) → 4-methyltrityl chloride (23429-44-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) Mg / 1) ether, 2) benzene

2: 90 percent / acetyl chloride / benzene / 1 h / Heating

With magnesium; acetyl chloride; In benzene;

DOI:10.1021/jo00026a024

Reference yield:

benzophenone (119-61-9) → 4-methyltrityl chloride (23429-44-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) Mg, (ii) /BRN= 1238185/

2: AcCl

With acetyl chloride;

DOI:10.1021/jo01323a020

upstream raw materials:

(4-methylphenyl)diphenylmethanol

toluene

bromobenzene

4-Methylbenzophenone

Downstream raw materials:

C₄₀H₃₄

C₂₇H₃₂N₂O₂

C₂₅H₂₈N₂O₂

C₄₃H₄₆N₈O₄